喹烯酮-D5同位素标准品

Analysis Method

Product Specification

Product Result

Chemical Purity by HPLC/UV

≥98%

99.42%

Identity by ¹H NMR

Conforms to Structure

Pass

Identity by ¹³C NMR

Conforms to Structure

Pass

Identity by Mass Spectrometry

Conforms to Structure

Pass

Isotope Incorporation by Mass Spectrometry

≥98% D/Molecule

99.68%

Intended Use

This material is intended only for laboratory use in analytical and R+D applications. It not suitable for human/animal consumption or for household use.

Hazards

Read Material Safety Data Sheet (MSDS) and understand any potential hazard(s) prior to the use of this product. All chemicals 首ld be considered potentially hazardous in nature and 首ld only be handled by qualified personnel using established good laboratory practices.

Instrument:

Shimadzu LCMS-2020

Column:

Eclipse XDB C18 4.6×250 mm, 5 μm

Mobile Phase:

A: 0.1% Formic acid in Water  B: Acetonitrile

Gradient:

88%B over 1 min, 88%～50%B from 1 min to 2 min, 50%～12%B from 2 min to 3.5 min, 12%～88% from 3.5 min to 4.5 min,maintain to 6 min

Flow Rate:

1.0 mL/min

Wavelength:

254nm

Acquisition Date:

December 6, 2018

Peak #

Ret. Time (min.)

Area (mAU)

Height (mAU)

Area %

1

2.602

17152

3592

0.576

2

2.755

2959140

627997

99.424

Total

2976292

631589

100.000

Instrument:

Bruker ANANCE 600MHz

Solvent:

CDCl₃

Acquisition Date:

December 6, 2018